Specifications
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CRM State:
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Matrix:
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Mineralisation:
OREAS 703 was prepared from a blend of granodiorite, limestone, multiple
mineral concentrates (Mo, W, and Bi), and high-grade fluorite ore. The tungsten-
and bismuth-bearing concentrates were sourced from the Nui Phao polymetallic
deposit in northern Vietnam, which is characterised by skarn-hosted
mineralisation containing scheelite and bismuth sulphide minerals. The resulting
CRM is chemically representative of a polymetallic silicate–carbonate
system.
Twenty-five commercial analytical laboratories participated in the program to certify the elements reported below using the following methods:
Homogeneity was evaluated using 12 subsamples analysed by oxidising fusion with X-ray fluorescence finish. ANOVA was applied to duplicates from six test units to compare within- and between-unit variances, providing a statistical measure of batch homogeneity.
| Analyte | Certified Value | 1SD | Expanded Uncertainty Low | Expanded Uncertainty High | Method |
|---|---|---|---|---|---|
| WO3, Tungsten trioxide (wt.%) | 0.634 | 0.056 | 0.602 | 0.666 | Borate / Peroxide Fusion ICP |
| Bi, Bismuth (ppm) | 541 | 33 | 515 | 568 | Borate / Peroxide Fusion ICP |
| Mo, Molybdenum (ppm) | 1026 | 73 | 980 | 1072 | Borate / Peroxide Fusion ICP |
| F, Fluorine (wt.%) | 0.621 | 0.103 | 0.556 | 0.686 | Ion Selective Electrode |
| WO3, Tungsten trioxide (wt.%) | 0.625 | 0.012 | 0.614 | 0.637 | Borate Fusion XRF |
| Al2O3, Aluminium(III) oxide (wt.%) | 10.36 | 0.132 | 10.25 | 10.47 | Borate Fusion XRF |
| As, Arsenic (ppm) | < 100 | IND | IND | IND | Borate Fusion XRF |
| BaO, Barium oxide (ppm) | 788 | 80 | 691 | 884 | Borate Fusion XRF |
| Bi, Bismuth (ppm) | 570 | 75 | 513 | 628 | Borate Fusion XRF |
| CaO, Calcium oxide (wt.%) | 19.21 | 0.209 | 19.06 | 19.37 | Borate Fusion XRF |
| Co, Cobalt (ppm) | < 100 | IND | IND | IND | Borate Fusion XRF |
| Cr2O3, Chromium(III) oxide (ppm) | < 150 | IND | IND | IND | Borate Fusion XRF |
| Cu, Copper (ppm) | 715 | 35 | 684 | 747 | Borate Fusion XRF |
| Fe2O3, Iron(III) oxide (wt.%) | 4.27 | 0.081 | 4.21 | 4.33 | Borate Fusion XRF |
| HfO2, Hafnium dioxide (ppm) | < 100 | IND | IND | IND | Borate Fusion XRF |
| K2O, Potassium oxide (wt.%) | 2.46 | 0.049 | 2.42 | 2.49 | Borate Fusion XRF |
| MgO, Magnesium oxide (wt.%) | 1.05 | 0.030 | 1.03 | 1.07 | Borate Fusion XRF |
| MnO, Manganese oxide (wt.%) | 0.050 | 0.005 | 0.046 | 0.054 | Borate Fusion XRF |
| Mo, Molybdenum (ppm) | 1083 | 70 | 1004 | 1163 | Borate Fusion XRF |
| Na2O, Sodium oxide (wt.%) | 1.90 | 0.105 | 1.83 | 1.97 | Borate Fusion XRF |
| Ni, Nickel (ppm) | < 50 | IND | IND | IND | Borate Fusion XRF |
| P2O5, Phosphorus(V) oxide (wt.%) | 0.139 | 0.003 | 0.136 | 0.142 | Borate Fusion XRF |
| Pb, Lead (ppm) | < 50 | IND | IND | IND | Borate Fusion XRF |
| SiO2, Silicon dioxide (wt.%) | 44.86 | 0.403 | 44.42 | 45.30 | Borate Fusion XRF |
| SO3, Sulphur trioxide (wt.%) | 1.63 | 0.062 | 1.57 | 1.69 | Borate Fusion XRF |
| Sr, Strontium (ppm) | 184 | 40 | 135 | 233 | Borate Fusion XRF |
| TiO2, Titanium dioxide (wt.%) | 0.416 | 0.018 | 0.402 | 0.430 | Borate Fusion XRF |
| Zn, Zinc (ppm) | 71 | 18 | 51 | 91 | Borate Fusion XRF |
| LOI1000, Loss on ignition @1000 °C (wt.%) | 12.75 | 0.245 | 12.56 | 12.94 | Thermogravimetry |
| S, Sulphur (wt.%) | 0.654 | 0.025 | 0.636 | 0.672 | Infrared Combustion |
| Al2O3, Aluminium(III) oxide (wt.%) | 10.35 | 0.228 | 10.11 | 10.59 | Borate / Peroxide Fusion ICP |
| Ba, Barium (ppm) | 708 | 18 | 685 | 731 | Borate / Peroxide Fusion ICP |
| Be, Beryllium (ppm) | 10.3 | 1.2 | 9.3 | 11.3 | Borate / Peroxide Fusion ICP |
| CaO, Calcium oxide (wt.%) | 19.17 | 0.667 | 18.65 | 19.68 | Borate / Peroxide Fusion ICP |
| Cd, Cadmium (ppm) | < 10.0 | IND | IND | IND | Borate / Peroxide Fusion ICP |
| Ce, Cerium (ppm) | 66 | 2.9 | 63 | 69 | Borate / Peroxide Fusion ICP |
| Co, Cobalt (ppm) | 8.23 | 0.92 | 7.27 | 9.19 | Borate / Peroxide Fusion ICP |
| Cr, Chromium (ppm) | 33.0 | 2.97 | 29.4 | 36.6 | Borate / Peroxide Fusion ICP |
| Cs, Caesium (ppm) | 10.1 | 0.63 | 9.6 | 10.7 | Borate / Peroxide Fusion ICP |
| Cu, Copper (ppm) | 727 | 46 | 686 | 767 | Borate / Peroxide Fusion ICP |
| Dy, Dysprosium (ppm) | 5.44 | 0.296 | 5.07 | 5.81 | Borate / Peroxide Fusion ICP |
| Er, Erbium (ppm) | 2.73 | 0.148 | 2.52 | 2.93 | Borate / Peroxide Fusion ICP |
| Eu, Europium (ppm) | 1.15 | 0.072 | 1.06 | 1.25 | Borate / Peroxide Fusion ICP |
| Fe2O3, Iron(III) oxide (wt.%) | 4.33 | 0.107 | 4.21 | 4.44 | Borate / Peroxide Fusion ICP |
| Ga, Gallium (ppm) | 16.1 | 0.50 | 15.5 | 16.7 | Borate / Peroxide Fusion ICP |
| Gd, Gadolinium (ppm) | 6.04 | 0.411 | 5.63 | 6.44 | Borate / Peroxide Fusion ICP |
| Hf, Hafnium (ppm) | 4.86 | 0.65 | 4.29 | 5.43 | Borate / Peroxide Fusion ICP |
| Ho, Holmium (ppm) | 1.00 | 0.060 | 0.92 | 1.08 | Borate / Peroxide Fusion ICP |
| K2O, Potassium oxide (wt.%) | 2.47 | 0.083 | 2.38 | 2.56 | Borate / Peroxide Fusion ICP |
| La, Lanthanum (ppm) | 33.5 | 1.37 | 32.0 | 35.1 | Borate / Peroxide Fusion ICP |
| Li, Lithium (ppm) | 42.2 | 3.11 | 38.7 | 45.6 | Borate / Peroxide Fusion ICP |
| Lu, Lutetium (ppm) | 0.35 | 0.031 | 0.31 | 0.38 | Borate / Peroxide Fusion ICP |
| MgO, Magnesium oxide (wt.%) | 1.04 | 0.039 | 1.01 | 1.07 | Borate / Peroxide Fusion ICP |
| MnO, Manganese oxide (wt.%) | 0.049 | 0.002 | 0.048 | 0.050 | Borate / Peroxide Fusion ICP |
| Na2O, Sodium oxide (wt.%) | 1.91 | 0.043 | 1.83 | 1.98 | Borate / Peroxide Fusion ICP |
| Nb, Niobium (ppm) | 9.63 | 0.459 | 9.05 | 10.21 | Borate / Peroxide Fusion ICP |
| Nd, Neodymium (ppm) | 29.9 | 1.74 | 27.9 | 31.9 | Borate / Peroxide Fusion ICP |
| P2O5, Phosphorus(V) oxide (wt.%) | 0.141 | 0.006 | 0.132 | 0.150 | Borate / Peroxide Fusion ICP |
| Pb, Lead (ppm) | 18.0 | 2.6 | 15.5 | 20.5 | Borate / Peroxide Fusion ICP |
| Pr, Praseodymium (ppm) | 7.87 | 0.399 | 7.41 | 8.34 | Borate / Peroxide Fusion ICP |
| Rb, Rubidium (ppm) | 135 | 6 | 130 | 139 | Borate / Peroxide Fusion ICP |
| S, Sulphur (wt.%) | 0.650 | 0.049 | 0.608 | 0.692 | Borate / Peroxide Fusion ICP |
| Sc, Scandium (ppm) | 6.47 | 0.564 | 5.49 | 7.45 | Borate / Peroxide Fusion ICP |
| SiO2, Silicon dioxide (wt.%) | 45.43 | 1.039 | 44.24 | 46.63 | Borate / Peroxide Fusion ICP |
| Sm, Samarium (ppm) | 6.40 | 0.385 | 5.97 | 6.83 | Borate / Peroxide Fusion ICP |
| Sn, Tin (ppm) | 5.98 | 0.503 | 5.24 | 6.73 | Borate / Peroxide Fusion ICP |
| Sr, Strontium (ppm) | 184 | 8 | 178 | 191 | Borate / Peroxide Fusion ICP |
| Ta, Tantalum (ppm) | 0.87 | 0.09 | 0.76 | 0.99 | Borate / Peroxide Fusion ICP |
| Tb, Terbium (ppm) | 0.93 | 0.048 | 0.87 | 1.00 | Borate / Peroxide Fusion ICP |
| Th, Thorium (ppm) | 10.7 | 0.52 | 10.0 | 11.4 | Borate / Peroxide Fusion ICP |
| Ti, Titanium (wt.%) | 0.252 | 0.011 | 0.244 | 0.259 | Borate / Peroxide Fusion ICP |
| Tl, Thallium (ppm) | 0.77 | 0.11 | 0.62 | 0.93 | Borate / Peroxide Fusion ICP |
| Tm, Thulium (ppm) | 0.37 | 0.028 | 0.34 | 0.40 | Borate / Peroxide Fusion ICP |
| U, Uranium (ppm) | 5.93 | 0.276 | 5.40 | 6.46 | Borate / Peroxide Fusion ICP |
| V, Vanadium (ppm) | 44.4 | 3.32 | 42.1 | 46.7 | Borate / Peroxide Fusion ICP |
| Y, Yttrium (ppm) | 26.5 | 2.03 | 24.8 | 28.1 | Borate / Peroxide Fusion ICP |
| Yb, Ytterbium (ppm) | 2.40 | 0.153 | 2.16 | 2.64 | Borate / Peroxide Fusion ICP |
| Zn, Zinc (ppm) | 69 | 8 | 60 | 79 | Borate / Peroxide Fusion ICP |
| Zr, Zirconium (ppm) | 186 | 11 | 172 | 199 | Borate / Peroxide Fusion ICP |
| Ag, Silver (ppm) | 0.292 | 0.027 | 0.261 | 0.322 | 4-Acid Digestion |
| Al, Aluminium (wt.%) | 5.46 | 0.128 | 5.26 | 5.66 | 4-Acid Digestion |
| As, Arsenic (ppm) | 3.48 | 0.38 | 2.80 | 4.15 | 4-Acid Digestion |
| Ba, Barium (ppm) | 709 | 16 | 687 | 732 | 4-Acid Digestion |
| Be, Beryllium (ppm) | 9.58 | 0.630 | 9.09 | 10.07 | 4-Acid Digestion |
| Bi, Bismuth (ppm) | 553 | 32 | 529 | 576 | 4-Acid Digestion |
| Ca, Calcium (wt.%) | 13.35 | 0.503 | 12.90 | 13.81 | 4-Acid Digestion |
| Ce, Cerium (ppm) | 70 | 4.1 | 65 | 74 | 4-Acid Digestion |
| Co, Cobalt (ppm) | 7.91 | 0.530 | 7.41 | 8.41 | 4-Acid Digestion |
| Cr, Chromium (ppm) | 24.7 | 2.6 | 21.9 | 27.5 | 4-Acid Digestion |
| Cs, Caesium (ppm) | 10.6 | 0.50 | 9.9 | 11.2 | 4-Acid Digestion |
| Cu, Copper (ppm) | 719 | 28 | 694 | 745 | 4-Acid Digestion |
| Dy, Dysprosium (ppm) | 4.02 | 0.180 | 3.67 | 4.37 | 4-Acid Digestion |
| Er, Erbium (ppm) | 1.69 | 0.064 | 1.55 | 1.83 | 4-Acid Digestion |
| Eu, Europium (ppm) | 1.18 | 0.065 | 1.07 | 1.30 | 4-Acid Digestion |
| Fe, Iron (wt.%) | 3.00 | 0.100 | 2.90 | 3.11 | 4-Acid Digestion |
| Ga, Gallium (ppm) | 15.7 | 0.67 | 14.9 | 16.5 | 4-Acid Digestion |
| Gd, Gadolinium (ppm) | 5.64 | 0.56 | 4.98 | 6.31 | 4-Acid Digestion |
| Hf, Hafnium (ppm) | 1.31 | 0.119 | 1.17 | 1.45 | 4-Acid Digestion |
| Ho, Holmium (ppm) | 0.67 | 0.051 | 0.60 | 0.75 | 4-Acid Digestion |
| In, Indium (ppm) | 0.16 | 0.010 | 0.15 | 0.17 | 4-Acid Digestion |
| K, Potassium (wt.%) | 2.05 | 0.060 | 1.99 | 2.12 | 4-Acid Digestion |
| La, Lanthanum (ppm) | 34.2 | 2.49 | 32.3 | 36.2 | 4-Acid Digestion |
| Li, Lithium (ppm) | 40.6 | 1.33 | 39.1 | 42.1 | 4-Acid Digestion |
| Lu, Lutetium (ppm) | 0.18 | 0.013 | 0.16 | 0.20 | 4-Acid Digestion |
| Mg, Magnesium (wt.%) | 0.606 | 0.024 | 0.587 | 0.625 | 4-Acid Digestion |
| Mn, Manganese (wt.%) | 0.036 | 0.001 | 0.035 | 0.037 | 4-Acid Digestion |
| Mo, Molybdenum (ppm) | 1020 | 45 | 986 | 1054 | 4-Acid Digestion |
| Na, Sodium (wt.%) | 1.41 | 0.032 | 1.35 | 1.46 | 4-Acid Digestion |
| Nb, Niobium (ppm) | 9.16 | 0.576 | 8.47 | 9.85 | 4-Acid Digestion |
| Nd, Neodymium (ppm) | 29.9 | 2.52 | 26.9 | 32.8 | 4-Acid Digestion |
| Ni, Nickel (ppm) | 11.8 | 0.81 | 10.8 | 12.9 | 4-Acid Digestion |
| P, Phosphorus (wt.%) | 0.061 | 0.002 | 0.058 | 0.063 | 4-Acid Digestion |
| Pb, Lead (ppm) | 18.5 | 1.67 | 17.2 | 19.8 | 4-Acid Digestion |
| Pr, Praseodymium (ppm) | 8.16 | 0.373 | 7.58 | 8.74 | 4-Acid Digestion |
| Rb, Rubidium (ppm) | 139 | 7 | 132 | 146 | 4-Acid Digestion |
| Re, Rhenium (ppm) | 0.064 | 0.015 | 0.049 | 0.080 | 4-Acid Digestion |
| S, Sulphur (wt.%) | 0.662 | 0.028 | 0.637 | 0.687 | 4-Acid Digestion |
| Sb, Antimony (ppm) | 0.53 | 0.048 | 0.45 | 0.61 | 4-Acid Digestion |
| Sc, Scandium (ppm) | 6.02 | 0.375 | 5.68 | 6.35 | 4-Acid Digestion |
| Sm, Samarium (ppm) | 6.15 | 0.80 | 5.29 | 7.01 | 4-Acid Digestion |
| Sn, Tin (ppm) | 5.58 | 0.165 | 5.32 | 5.84 | 4-Acid Digestion |
| Sr, Strontium (ppm) | 186 | 6 | 179 | 193 | 4-Acid Digestion |
| Ta, Tantalum (ppm) | 0.65 | 0.17 | 0.47 | 0.83 | 4-Acid Digestion |
| Tb, Terbium (ppm) | 0.81 | 0.051 | 0.73 | 0.88 | 4-Acid Digestion |
| Te, Tellurium (ppm) | 2.14 | 0.25 | 1.88 | 2.40 | 4-Acid Digestion |
| Th, Thorium (ppm) | 10.9 | 0.73 | 10.1 | 11.7 | 4-Acid Digestion |
| Ti, Titanium (wt.%) | 0.245 | 0.006 | 0.236 | 0.254 | 4-Acid Digestion |
| Tl, Thallium (ppm) | 0.80 | 0.038 | 0.76 | 0.84 | 4-Acid Digestion |
| Tm, Thulium (ppm) | 0.22 | 0.013 | 0.19 | 0.24 | 4-Acid Digestion |
| U, Uranium (ppm) | 5.73 | 0.359 | 5.17 | 6.29 | 4-Acid Digestion |
| V, Vanadium (ppm) | 40.9 | 1.77 | 38.9 | 42.9 | 4-Acid Digestion |
| W, Tungsten (wt.%) | 0.459 | 0.050 | 0.423 | 0.494 | 4-Acid Digestion |
| Y, Yttrium (ppm) | 16.5 | 1.31 | 15.6 | 17.3 | 4-Acid Digestion |
| Yb, Ytterbium (ppm) | 1.36 | 0.079 | 1.26 | 1.47 | 4-Acid Digestion |
| Zn, Zinc (ppm) | 68 | 2.0 | 65 | 71 | 4-Acid Digestion |
| Zr, Zirconium (ppm) | 41.8 | 4.8 | 38.0 | 45.6 | 4-Acid Digestion |