Specifications
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CRM State:
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Matrix:
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Mineralisation:
OREAS 702 was prepared from a blend of granodiorite, limestone, multiple
mineral concentrates (Mo, W, and Bi), and high-grade fluorite ore. The tungsten-
and bismuth-bearing concentrates were sourced from the Nui Phao polymetallic
deposit in northern Vietnam, which is characterised by skarn-hosted
mineralisation containing scheelite and bismuth sulphide minerals. The resulting
CRM is chemically representative of a polymetallic silicate–carbonate
system.
Twenty-five commercial analytical laboratories participated in the program to certify the elements reported below using the following methods:
Homogeneity was evaluated using 12 subsamples analysed by oxidising fusion with X-ray fluorescence finish. ANOVA was applied to duplicates from six test units to compare within- and between-unit variances, providing a statistical measure of batch homogeneity.
| Analyte | Certified Value | 1SD | Expanded Uncertainty Low | Expanded Uncertainty High | Method |
|---|---|---|---|---|---|
| WO3, Tungsten trioxide (wt.%) | 0.286 | 0.011 | 0.275 | 0.297 | Borate / Peroxide Fusion ICP |
| Bi, Bismuth (ppm) | 275 | 12 | 263 | 287 | Borate / Peroxide Fusion ICP |
| Mo, Molybdenum (ppm) | 588 | 41 | 558 | 617 | Borate / Peroxide Fusion ICP |
| F, Fluorine (wt.%) | 0.299 | 0.038 | 0.271 | 0.328 | Ion Selective Electrode |
| WO3, Tungsten trioxide (wt.%) | 0.277 | 0.007 | 0.271 | 0.283 | Borate Fusion XRF |
| Al2O3, Aluminium(III) oxide (wt.%) | 9.70 | 0.125 | 9.58 | 9.81 | Borate Fusion XRF |
| As, Arsenic (ppm) | < 100 | IND | IND | IND | Borate Fusion XRF |
| BaO, Barium oxide (ppm) | 738 | 49 | 668 | 808 | Borate Fusion XRF |
| Bi, Bismuth (ppm) | 287 | 53 | 238 | 336 | Borate Fusion XRF |
| CaO, Calcium oxide (wt.%) | 22.54 | 0.195 | 22.35 | 22.73 | Borate Fusion XRF |
| Co, Cobalt (ppm) | < 100 | IND | IND | IND | Borate Fusion XRF |
| Cr2O3, Chromium(III) oxide (ppm) | < 150 | IND | IND | IND | Borate Fusion XRF |
| Cu, Copper (ppm) | 352 | 18 | 329 | 375 | Borate Fusion XRF |
| Fe2O3, Iron(III) oxide (wt.%) | 3.36 | 0.081 | 3.31 | 3.41 | Borate Fusion XRF |
| HfO2, Hafnium dioxide (ppm) | < 100 | IND | IND | IND | Borate Fusion XRF |
| K2O, Potassium oxide (wt.%) | 2.27 | 0.032 | 2.24 | 2.30 | Borate Fusion XRF |
| MgO, Magnesium oxide (wt.%) | 1.03 | 0.029 | 1.00 | 1.06 | Borate Fusion XRF |
| MnO, Manganese oxide (wt.%) | 0.038 | 0.006 | 0.035 | 0.042 | Borate Fusion XRF |
| Mo, Molybdenum (ppm) | 625 | 35 | 585 | 666 | Borate Fusion XRF |
| Na2O, Sodium oxide (wt.%) | 1.77 | 0.073 | 1.72 | 1.82 | Borate Fusion XRF |
| Ni, Nickel (ppm) | < 50 | IND | IND | IND | Borate Fusion XRF |
| P2O5, Phosphorus(V) oxide (wt.%) | 0.129 | 0.006 | 0.122 | 0.136 | Borate Fusion XRF |
| Pb, Lead (ppm) | < 50 | IND | IND | IND | Borate Fusion XRF |
| SiO2, Silicon dioxide (wt.%) | 41.41 | 0.345 | 41.08 | 41.74 | Borate Fusion XRF |
| SO3, Sulphur trioxide (wt.%) | 0.906 | 0.019 | 0.879 | 0.934 | Borate Fusion XRF |
| Sr, Strontium (ppm) | 196 | 7 | 186 | 206 | Borate Fusion XRF |
| TiO2, Titanium dioxide (wt.%) | 0.386 | 0.013 | 0.374 | 0.398 | Borate Fusion XRF |
| Zn, Zinc (ppm) | 60 | 6 | 47 | 73 | Borate Fusion XRF |
| LOI1000, Loss on ignition @1000 °C (wt.%) | 16.06 | 0.073 | 15.97 | 16.15 | Thermogravimetry |
| S, Sulphur (wt.%) | 0.349 | 0.014 | 0.334 | 0.363 | Infrared Combustion |
| Al2O3, Aluminium(III) oxide (wt.%) | 9.56 | 0.152 | 9.32 | 9.81 | Borate / Peroxide Fusion ICP |
| Ba, Barium (ppm) | 650 | 18 | 631 | 669 | Borate / Peroxide Fusion ICP |
| Be, Beryllium (ppm) | 5.63 | 0.78 | 4.73 | 6.53 | Borate / Peroxide Fusion ICP |
| CaO, Calcium oxide (wt.%) | 22.21 | 0.695 | 21.68 | 22.75 | Borate / Peroxide Fusion ICP |
| Cd, Cadmium (ppm) | < 10.0 | IND | IND | IND | Borate / Peroxide Fusion ICP |
| Ce, Cerium (ppm) | 56 | 2.6 | 53 | 59 | Borate / Peroxide Fusion ICP |
| Co, Cobalt (ppm) | 6.74 | 0.71 | 5.90 | 7.58 | Borate / Peroxide Fusion ICP |
| Cr, Chromium (ppm) | 29.5 | 3.9 | 24.5 | 34.4 | Borate / Peroxide Fusion ICP |
| Cs, Caesium (ppm) | 8.53 | 0.514 | 8.05 | 9.01 | Borate / Peroxide Fusion ICP |
| Cu, Copper (ppm) | 362 | 23 | 341 | 383 | Borate / Peroxide Fusion ICP |
| Dy, Dysprosium (ppm) | 4.46 | 0.294 | 3.99 | 4.92 | Borate / Peroxide Fusion ICP |
| Er, Erbium (ppm) | 2.26 | 0.161 | 2.05 | 2.48 | Borate / Peroxide Fusion ICP |
| Eu, Europium (ppm) | 1.01 | 0.073 | 0.89 | 1.13 | Borate / Peroxide Fusion ICP |
| Fe2O3, Iron(III) oxide (wt.%) | 3.38 | 0.088 | 3.29 | 3.48 | Borate / Peroxide Fusion ICP |
| Ga, Gallium (ppm) | 14.2 | 0.60 | 13.5 | 15.0 | Borate / Peroxide Fusion ICP |
| Gd, Gadolinium (ppm) | 5.07 | 0.309 | 4.74 | 5.41 | Borate / Peroxide Fusion ICP |
| Hf, Hafnium (ppm) | 4.52 | 0.308 | 4.08 | 4.97 | Borate / Peroxide Fusion ICP |
| Ho, Holmium (ppm) | 0.84 | 0.074 | 0.76 | 0.92 | Borate / Peroxide Fusion ICP |
| K2O, Potassium oxide (wt.%) | 2.32 | 0.080 | 2.24 | 2.39 | Borate / Peroxide Fusion ICP |
| La, Lanthanum (ppm) | 27.8 | 1.13 | 26.3 | 29.3 | Borate / Peroxide Fusion ICP |
| Li, Lithium (ppm) | 37.9 | 3.38 | 34.7 | 41.2 | Borate / Peroxide Fusion ICP |
| Lu, Lutetium (ppm) | 0.29 | 0.023 | 0.25 | 0.32 | Borate / Peroxide Fusion ICP |
| MgO, Magnesium oxide (wt.%) | 1.01 | 0.045 | 0.97 | 1.04 | Borate / Peroxide Fusion ICP |
| MnO, Manganese oxide (wt.%) | 0.040 | 0.001 | 0.039 | 0.041 | Borate / Peroxide Fusion ICP |
| Na2O, Sodium oxide (wt.%) | 1.77 | 0.043 | 1.70 | 1.84 | Borate / Peroxide Fusion ICP |
| Nb, Niobium (ppm) | 8.78 | 0.462 | 8.02 | 9.53 | Borate / Peroxide Fusion ICP |
| Nd, Neodymium (ppm) | 25.7 | 1.35 | 23.8 | 27.5 | Borate / Peroxide Fusion ICP |
| P2O5, Phosphorus(V) oxide (wt.%) | 0.133 | 0.005 | 0.125 | 0.141 | Borate / Peroxide Fusion ICP |
| Pb, Lead (ppm) | 17.6 | 2.9 | 15.0 | 20.1 | Borate / Peroxide Fusion ICP |
| Pr, Praseodymium (ppm) | 6.71 | 0.363 | 6.24 | 7.19 | Borate / Peroxide Fusion ICP |
| Rb, Rubidium (ppm) | 120 | 4 | 115 | 124 | Borate / Peroxide Fusion ICP |
| S, Sulphur (wt.%) | 0.346 | 0.029 | 0.315 | 0.377 | Borate / Peroxide Fusion ICP |
| Sc, Scandium (ppm) | 5.81 | 0.439 | 5.30 | 6.32 | Borate / Peroxide Fusion ICP |
| SiO2, Silicon dioxide (wt.%) | 42.01 | 0.876 | 40.87 | 43.15 | Borate / Peroxide Fusion ICP |
| Sm, Samarium (ppm) | 5.60 | 0.380 | 5.12 | 6.07 | Borate / Peroxide Fusion ICP |
| Sn, Tin (ppm) | 4.36 | 0.298 | 3.84 | 4.87 | Borate / Peroxide Fusion ICP |
| Sr, Strontium (ppm) | 195 | 10 | 188 | 202 | Borate / Peroxide Fusion ICP |
| Ta, Tantalum (ppm) | 0.78 | 0.16 | 0.65 | 0.92 | Borate / Peroxide Fusion ICP |
| Tb, Terbium (ppm) | 0.78 | 0.050 | 0.72 | 0.85 | Borate / Peroxide Fusion ICP |
| Th, Thorium (ppm) | 9.88 | 0.502 | 9.14 | 10.61 | Borate / Peroxide Fusion ICP |
| Ti, Titanium (wt.%) | 0.237 | 0.009 | 0.230 | 0.245 | Borate / Peroxide Fusion ICP |
| Tl, Thallium (ppm) | 0.70 | 0.07 | 0.60 | 0.80 | Borate / Peroxide Fusion ICP |
| Tm, Thulium (ppm) | 0.31 | 0.019 | 0.29 | 0.34 | Borate / Peroxide Fusion ICP |
| U, Uranium (ppm) | 4.20 | 0.44 | 3.66 | 4.73 | Borate / Peroxide Fusion ICP |
| V, Vanadium (ppm) | 41.6 | 2.83 | 39.3 | 44.0 | Borate / Peroxide Fusion ICP |
| Y, Yttrium (ppm) | 22.8 | 1.67 | 21.3 | 24.3 | Borate / Peroxide Fusion ICP |
| Yb, Ytterbium (ppm) | 1.99 | 0.161 | 1.74 | 2.25 | Borate / Peroxide Fusion ICP |
| Zn, Zinc (ppm) | 59 | 6 | 53 | 65 | Borate / Peroxide Fusion ICP |
| Zr, Zirconium (ppm) | 167 | 8 | 158 | 177 | Borate / Peroxide Fusion ICP |
| Ag, Silver (ppm) | 0.178 | 0.016 | 0.156 | 0.201 | 4-Acid Digestion |
| Al, Aluminium (wt.%) | 5.10 | 0.111 | 4.99 | 5.22 | 4-Acid Digestion |
| As, Arsenic (ppm) | 3.54 | 0.75 | 2.70 | 4.39 | 4-Acid Digestion |
| Ba, Barium (ppm) | 657 | 15 | 634 | 679 | 4-Acid Digestion |
| Be, Beryllium (ppm) | 5.24 | 0.375 | 5.00 | 5.48 | 4-Acid Digestion |
| Bi, Bismuth (ppm) | 277 | 21 | 264 | 291 | 4-Acid Digestion |
| Ca, Calcium (wt.%) | 15.63 | 0.608 | 15.10 | 16.17 | 4-Acid Digestion |
| Ce, Cerium (ppm) | 59 | 3.1 | 56 | 63 | 4-Acid Digestion |
| Co, Cobalt (ppm) | 6.47 | 0.450 | 6.02 | 6.93 | 4-Acid Digestion |
| Cr, Chromium (ppm) | 21.4 | 3.0 | 19.2 | 23.6 | 4-Acid Digestion |
| Cs, Caesium (ppm) | 8.77 | 0.513 | 8.27 | 9.28 | 4-Acid Digestion |
| Cu, Copper (ppm) | 358 | 16 | 346 | 370 | 4-Acid Digestion |
| Dy, Dysprosium (ppm) | 3.18 | 0.201 | 2.89 | 3.47 | 4-Acid Digestion |
| Er, Erbium (ppm) | 1.26 | 0.054 | 1.17 | 1.36 | 4-Acid Digestion |
| Eu, Europium (ppm) | 1.06 | 0.068 | 0.94 | 1.17 | 4-Acid Digestion |
| Fe, Iron (wt.%) | 2.34 | 0.061 | 2.27 | 2.40 | 4-Acid Digestion |
| Ga, Gallium (ppm) | 14.0 | 0.78 | 13.2 | 14.8 | 4-Acid Digestion |
| Gd, Gadolinium (ppm) | 4.52 | 0.374 | 4.04 | 4.99 | 4-Acid Digestion |
| Hf, Hafnium (ppm) | 1.26 | 0.16 | 1.09 | 1.43 | 4-Acid Digestion |
| Ho, Holmium (ppm) | 0.50 | 0.05 | 0.44 | 0.57 | 4-Acid Digestion |
| In, Indium (ppm) | 0.097 | 0.008 | 0.087 | 0.108 | 4-Acid Digestion |
| K, Potassium (wt.%) | 1.91 | 0.049 | 1.86 | 1.96 | 4-Acid Digestion |
| La, Lanthanum (ppm) | 28.8 | 2.05 | 27.0 | 30.6 | 4-Acid Digestion |
| Li, Lithium (ppm) | 36.9 | 1.64 | 35.2 | 38.6 | 4-Acid Digestion |
| Lu, Lutetium (ppm) | 0.14 | 0.013 | 0.12 | 0.16 | 4-Acid Digestion |
| Mg, Magnesium (wt.%) | 0.587 | 0.025 | 0.565 | 0.608 | 4-Acid Digestion |
| Mn, Manganese (wt.%) | 0.031 | 0.001 | 0.030 | 0.032 | 4-Acid Digestion |
| Mo, Molybdenum (ppm) | 577 | 32 | 557 | 597 | 4-Acid Digestion |
| Na, Sodium (wt.%) | 1.32 | 0.023 | 1.28 | 1.36 | 4-Acid Digestion |
| Nb, Niobium (ppm) | 8.68 | 0.383 | 8.23 | 9.14 | 4-Acid Digestion |
| Nd, Neodymium (ppm) | 24.8 | 3.2 | 21.8 | 27.8 | 4-Acid Digestion |
| Ni, Nickel (ppm) | 11.3 | 0.76 | 10.6 | 12.0 | 4-Acid Digestion |
| P, Phosphorus (wt.%) | 0.058 | 0.002 | 0.055 | 0.060 | 4-Acid Digestion |
| Pb, Lead (ppm) | 17.3 | 1.49 | 16.1 | 18.5 | 4-Acid Digestion |
| Pr, Praseodymium (ppm) | 6.89 | 0.355 | 6.34 | 7.45 | 4-Acid Digestion |
| Rb, Rubidium (ppm) | 123 | 5 | 118 | 129 | 4-Acid Digestion |
| Re, Rhenium (ppm) | 0.035 | 0.008 | 0.028 | 0.042 | 4-Acid Digestion |
| S, Sulphur (wt.%) | 0.349 | 0.021 | 0.334 | 0.365 | 4-Acid Digestion |
| Sb, Antimony (ppm) | 0.37 | 0.05 | 0.31 | 0.42 | 4-Acid Digestion |
| Sc, Scandium (ppm) | 5.62 | 0.326 | 5.28 | 5.96 | 4-Acid Digestion |
| Sm, Samarium (ppm) | 5.17 | 0.66 | 4.47 | 5.87 | 4-Acid Digestion |
| Sn, Tin (ppm) | 4.10 | 0.109 | 3.91 | 4.29 | 4-Acid Digestion |
| Sr, Strontium (ppm) | 198 | 8 | 191 | 204 | 4-Acid Digestion |
| Ta, Tantalum (ppm) | 0.72 | 0.070 | 0.66 | 0.79 | 4-Acid Digestion |
| Tb, Terbium (ppm) | 0.66 | 0.050 | 0.58 | 0.74 | 4-Acid Digestion |
| Te, Tellurium (ppm) | 1.13 | 0.13 | 0.96 | 1.29 | 4-Acid Digestion |
| Th, Thorium (ppm) | 10.0 | 0.50 | 9.3 | 10.7 | 4-Acid Digestion |
| Ti, Titanium (wt.%) | 0.230 | 0.009 | 0.222 | 0.238 | 4-Acid Digestion |
| Tl, Thallium (ppm) | 0.71 | 0.038 | 0.66 | 0.75 | 4-Acid Digestion |
| Tm, Thulium (ppm) | 0.17 | 0.013 | 0.14 | 0.20 | 4-Acid Digestion |
| U, Uranium (ppm) | 3.93 | 0.372 | 3.42 | 4.44 | 4-Acid Digestion |
| V, Vanadium (ppm) | 38.5 | 1.55 | 36.9 | 40.0 | 4-Acid Digestion |
| W, Tungsten (wt.%) | 0.215 | 0.014 | 0.206 | 0.224 | 4-Acid Digestion |
| Y, Yttrium (ppm) | 13.1 | 1.3 | 12.2 | 13.9 | 4-Acid Digestion |
| Yb, Ytterbium (ppm) | 1.03 | 0.051 | 0.92 | 1.14 | 4-Acid Digestion |
| Zn, Zinc (ppm) | 57 | 2.8 | 54 | 60 | 4-Acid Digestion |
| Zr, Zirconium (ppm) | 40.0 | 3.92 | 36.5 | 43.5 | 4-Acid Digestion |